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BITSAT2020ChemistryGeneral Organic ChemistryActual

The Lassaigne's extract is boiled with dil. HNO ₃ before testing for halogens because

Options

  1. Asilver halides are soluble in HNO ₃
  2. BNa ₂ ~S and NaCN are decomposed by HNO ₃
  3. CAg ₂ ~S is soluble in HNO ₃
  4. DAgCN is soluble in HNO ₃

Correct answer

B. Na ₂ ~S and NaCN are decomposed by HNO ₃

Step-by-step solution

Na ₂ ~S and NaCN , formed during fusion with metallic sodium, must be removed before adding AgNO ₃, otherwise black ppt. due to Na ₂ ~S or white precipitate due to AgCN will be formed and thus white precipitate of AgCl will not be identified easily. Na ₂ ~S +2 AgNO ₃ 2 NaNO ₃+ Black Ag ₂ ~S NaCN + AgNO ₃ NaNO ₃ + White Ag CN NaCl + AgNO ₃ NaNO ₃+ White Ag Cl Na ₂ ~S +2 HNO ₃ boil 2 NaNO ₃+ H ₂ ~S NaCN + HNO ₃ boil NaNO ₃+ HCN

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