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JEE MainChemistryGeneral Organic Chemistry

Consider the two isomeric products formed when phenol reacts with dilute nitric acid at 298 K . Which of the following statements regarding the physical properties and separation of these isomers is INCORRECT?

Options

  1. AThe mixture of these isomers can be efficiently separated by steam distillation.
  2. Bo -nitrophenol is more soluble in water than p -nitrophenol.
  3. Co -nitrophenol has a lower boiling point than p -nitrophenol.
  4. Dp -nitrophenol is less volatile in steam due to intermolecular hydrogen bonding.

Correct answer

B. o -nitrophenol is more soluble in water than p -nitrophenol.

Step-by-step solution

The reaction of phenol with dilute HNO ₃ at 298 K yields o -nitrophenol and p -nitrophenol. o -nitrophenol exhibits intramolecular hydrogen bonding (chelation). This prevents the molecules from associating with each other, resulting in a lower boiling point and making it steam volatile. Furthermore, because its polar groups are involved in internal hydrogen bonding, they are less available to form hydrogen bonds with water, making o -nitrophenol less soluble in water. p -nitrophenol exhibits intermolecular hydrogen

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